TETRAPHENYLPHOSPHONIUM TETRAPHENYLBORATE
tetraphenylphosphonium tetraphenylborate
CAS: 15525-15-2
Molecular Formula: C48H40BP
TETRAPHENYLPHOSPHONIUM TETRAPHENYLBORATE - Names and Identifiers
| Name | tetraphenylphosphonium tetraphenylborate |
| Synonyms | TETRAPHENYLPHOSPHONI TETRAPHENYLBORON TETRAPHENYLPHOSPHONIUM TeTraphenylphosphonium TTraphenyl boraTe Tetraphenylphosphorium tetraphenylborate TETRAPHENYLPHOSPHONIUM TETRAPHENYLBORATE tetraphenylphosphonium tetraphenylborate TETRAPHENYLPHOSPHONIUM TETRAPHENYLBORATE TETRAPHENYLPHOSPHONIUM TETRAPHENYLBORATE |
| CAS | 15525-15-2 |
| InChI | InChI=1/C24H20B.C24H20P/c2*1-5-13-21(14-6-1)25(22-15-7-2-8-16-22,23-17-9-3-10-18-23)24-19-11-4-12-20-24/h2*1-20H/q-1;+1 |
TETRAPHENYLPHOSPHONIUM TETRAPHENYLBORATE - Physico-chemical Properties
| Molecular Formula | C48H40BP |
| Molar Mass | 658.62 |
| Melting Point | approximate 305℃ |
| Boling Point | 325-330 ℃(lit.) |
| Water Solubility | Insoluble in water |
| Appearance | powder to crystal |
| Color | White to Almost white |
| BRN | 3890798 |
| Storage Condition | Inert atmosphere,Room Temperature |
TETRAPHENYLPHOSPHONIUM TETRAPHENYLBORATE - Risk and Safety
| Safety Description | S22 - Do not breathe dust. S24/25 - Avoid contact with skin and eyes. |
| WGK Germany | 3 |
| FLUKA BRAND F CODES | 8 |
TETRAPHENYLPHOSPHONIUM TETRAPHENYLBORATE - Introduction
tetraphenylphosphonium tetraphenylborate (abbreviated as TPBP) is an organic compound. Its molecular formulas are C44H36BPH and C44H36BP, and its structure is characterized by a boron atom connected to four phenyl groups and a phosphine group. The following is a description of the nature, use, preparation and safety information of TPBP.
Nature:
-Appearance: TPBP is a solid, common color is white to light yellow.
-Melting point: Its melting point range is between 180-185°C.
-Solubility: TPBP has good solubility in common organic solvents, such as chloroform, dimethylformamide, etc.
Use:
-Catalyst: TPBP is commonly used as a ligand catalyst and can be used in organic synthesis reactions, such as hydrogenation reactions, oxidation reactions and sulfation reactions.
-Material synthesis: Because TPBP has a controllable size and shape, it has potential application value in the preparation of metal organic frameworks (MOF) and nanomaterials.
Method:
The preparation of TPBP usually uses a two-step reaction:
1. First, phenyl borohydride is generated by the reaction of phenyl borate and sodium borohydride.
2. Then react phenyl borohydride with phosphine compound to generate TPBP.
Safety Information:
- TPBP has a stimulating effect on the skin and eyes, so you should pay attention to protective measures when using it to avoid skin contact and eye exposure.
-Avoid dust fog or aerosols when handling TPBP to prevent inhalation.
- TPBP should be stored with strong oxidants and high temperatures to avoid dangerous situations such as combustion or explosion.
Please note that the use and handling of chemical substances need to follow the laboratory's safe operating procedures, implement appropriate laboratory safety measures, and read and follow the safety data sheets of relevant materials.
Nature:
-Appearance: TPBP is a solid, common color is white to light yellow.
-Melting point: Its melting point range is between 180-185°C.
-Solubility: TPBP has good solubility in common organic solvents, such as chloroform, dimethylformamide, etc.
Use:
-Catalyst: TPBP is commonly used as a ligand catalyst and can be used in organic synthesis reactions, such as hydrogenation reactions, oxidation reactions and sulfation reactions.
-Material synthesis: Because TPBP has a controllable size and shape, it has potential application value in the preparation of metal organic frameworks (MOF) and nanomaterials.
Method:
The preparation of TPBP usually uses a two-step reaction:
1. First, phenyl borohydride is generated by the reaction of phenyl borate and sodium borohydride.
2. Then react phenyl borohydride with phosphine compound to generate TPBP.
Safety Information:
- TPBP has a stimulating effect on the skin and eyes, so you should pay attention to protective measures when using it to avoid skin contact and eye exposure.
-Avoid dust fog or aerosols when handling TPBP to prevent inhalation.
- TPBP should be stored with strong oxidants and high temperatures to avoid dangerous situations such as combustion or explosion.
Please note that the use and handling of chemical substances need to follow the laboratory's safe operating procedures, implement appropriate laboratory safety measures, and read and follow the safety data sheets of relevant materials.
Last Update：2024-04-10 22:29:15
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